4--2,3,4,9-tetrahydro-1H-carbazol-1-one

Base Information

Chemical Name:4--2,3,4,9-tetrahydro-1H-carbazol-1-one
CAS No.:174625-04-8
Molecular Formula:C₂₁H₂₀N₂O₃
Molecular Weight:348.401
Hs Code.:

4-<benzoyl-(2-hydroxyethyl)amino>-2,3,4,9-tetrahydro-1H-carbazol-1-one

Synonyms:4--2,3,4,9-tetrahydro-1H-carbazol-1-one

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Chemical Property of 4--2,3,4,9-tetrahydro-1H-carbazol-1-one

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Technology Process of 4--2,3,4,9-tetrahydro-1H-carbazol-1-one

There total 7 articles about 4--2,3,4,9-tetrahydro-1H-carbazol-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 197178-32-8
4-[benzoyl(2-benzyloxyethyl)amino]-2,3,4,9-tetrahydro-1H-carbazol-1-one

: 174625-04-8
4--2,3,4,9-tetrahydro-1H-carbazol-1-one

Guidance literature:: With hydrogen; palladium dihydroxide; In tetrahydrofuran; for 20h; Ambient temperature;
DOI:10.1002/jhet.5570340423

Reference yield: 62.0%

: 174625-03-7
N-benzoyl-N-(2-hydroxyethyl)-(2,3,4,9-tetrahydrospiro<1H-carbazole-1,2'-(1,3)dithiolan>-4-yl)amine

: 174625-04-8
4--2,3,4,9-tetrahydro-1H-carbazol-1-one

Guidance literature:: With pyridine; benzeneseleninic anhydride; In chloroform; for 48h; Ambient temperature;
DOI:10.3987/COM-95-7060

Reference yield:

: 153231-38-0
2,3-Dihydrospiro(1H-carbazol-1,2'-[1,3]dithiolan)-4(9H)-on

: 174625-04-8
4--2,3,4,9-tetrahydro-1H-carbazol-1-one

Guidance literature:: Multi-step reaction with 5 steps

1: ferric chloride / benzene / 12 h / Heating

2: NaBH₄ / ethanol; tetrahydrofuran / 7 h

3: Et₃N / CHCl₃ / 0.5 h / Ambient temperature

4: 1.2 g / benzeneseleninic anhydride / CHCl₃ / 48 h / Ambient temperature

5: 64 percent / H₂ / 20percent Pd(OH)2 / tetrahydrofuran / 20 h / Ambient temperature

With sodium tetrahydroborate; benzeneseleninic anhydride; hydrogen; iron(III) chloride; triethylamine; palladium dihydroxide; In tetrahydrofuran; ethanol; chloroform; benzene;
DOI:10.1002/jhet.5570340423