C₁₇H₁₆F₆O₂

Base Information

Chemical Name:C₁₇H₁₆F₆O₂
CAS No.:1007592-12-2
Molecular Formula:C₁₇H₁₆F₆O₂
Molecular Weight:366.303
Hs Code.:

C<sub>17</sub>H<sub>16</sub>F<sub>6</sub>O<sub>2</sub>

Synonyms:C₁₇H₁₆F₆O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₆F₆O₂

Chemical Property:

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Technology Process of C₁₇H₁₆F₆O₂

There total 8 articles about C₁₇H₁₆F₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1007591-98-1
C₁₆H₁₃F₆NO

: 917-54-4
methyllithium

: 1007592-12-2
C₁₇H₁₆F₆O₂

Guidance literature:: C₁₆H₁₃F₆NO; methyllithium; In diethyl ether; tert-butyl methyl ether; at 0 - 5 ℃; for 1h;

With phosphoric acid; water; trifluoroacetic acid; In diethyl ether; tert-butyl methyl ether; at -70 - 20 ℃; for 0.5h;

With sodium carbonate; In tert-butyl methyl ether; water; Product distribution / selectivity;

Reference yield: 55.0%

: 1007594-35-5
C₁₈H₁₆O₃

: 368-63-8,68120-60-5,127852-28-2
(R)-[3,5-bis(trifluoromethyl)phenyl]ethanol

: 1007592-12-2
C₁₇H₁₆F₆O₂

Guidance literature:: With diethylzinc; palladium diacetate; 1,4-di(diphenylphosphino)-butane; Product distribution / selectivity;

Reference yield:

: 1007591-88-9
(S)-3-hydroxycyclopent-1-enecarbonitrile

: 1007592-12-2
C₁₇H₁₆F₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: diethylzinc / tetrahydrofuran; hexane / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: diethyl ether; tert-butyl methyl ether / 1 h / 0 °C / Inert atmosphere

3.2: -70 - -40 °C / Inert atmosphere

3.3: -40 - 20 °C / Inert atmosphere

With dmap; diethylzinc; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; tert-butyl methyl ether;
DOI:10.1021/ol1030348