{2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

Base Information

Chemical Name:{2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester
CAS No.:868140-88-9
Molecular Formula:C₂₄H₁₈BrF₅O₆
Molecular Weight:577.299
Hs Code.:

Synonyms:{2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

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Chemical Property of {2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

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Technology Process of {2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

There total 4 articles about {2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 868140-84-5
{2-[(7-methyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

: 868140-88-9
{2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 80 ℃; for 6h;
DOI:10.1021/jm0504297

Reference yield:

: 868140-80-1
{2-[(7-methyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid

: 868140-88-9
{2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / pyridine / dimethylformamide / 20 °C

2: 27 percent / N-bromosuccinimide; AIBN / CCl₄ / 6 h / 80 °C

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0504297

Reference yield:

: 23243-68-7,39927-08-7
3,6-dioxasuberic acid

: 868140-88-9
{2-[(7-bromomethyl-2-naphthyl)methoxycarbonylmethoxy]ethoxy}acetic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: aq. Cs₂CO₃ / methanol / 0.33 h / 20 °C

1.2: 46 mg / H₂O; dimethylformamide / 24 h / 70 °C

2.1: 53 percent / pyridine / dimethylformamide / 20 °C

3.1: 27 percent / N-bromosuccinimide; AIBN / CCl₄ / 6 h / 80 °C

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); caesium carbonate; In methanol; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0504297