1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

Base Information

Chemical Name:1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene
CAS No.:1037310-30-7
Molecular Formula:C₇₇H₈₀O₁₂
Molecular Weight:1197.47
Hs Code.:

Synonyms:1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

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Technology Process of 1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

There total 1 articles about 1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1037310-28-3
1,4-bis(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

: 100-44-7
benzyl chloride

: 1037310-30-7
1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

Guidance literature:: With potassium hydroxide; In water; at 100 ℃; for 5h;
DOI:10.1016/j.tet.2008.03.056

Reference yield:

: 1037310-30-7
1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: (-)-menthyl 2,3,4,6-tetra-O-benzyl-D-glucopyranoside

Guidance literature:: With NEt₄ClO₄; In dichloromethane; at 20 ℃; for 2.5h; Electrochemical reaction;
DOI:10.1016/j.tet.2008.03.056

Reference yield:

: 1037310-30-7
1,4-bis(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)-2,3,5-trimethylbenzene

: 6114-39-2,7309-59-3,82008-61-5,141-23-1
methyl 12-hydroxyoctadecanoate

: methyl 12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyloxy)octadecanoate

: 1037310-43-2
methyl 12-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)octadecanoate

Guidance literature:: With trifluorormethanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 2h; Title compound not separated from byproducts.;
DOI:10.1016/j.tet.2008.03.056