C₂₁H₂₇BrOS

Base Information

• Chemical Name: C₂₁H₂₇BrOS
• CAS No.: 1392504-20-9
• Molecular Formula: C₂₁H₂₇BrOS
• Molecular Weight: 407.415
• Mol file: 1392504-20-9.mol

Synonyms:C₂₁H₂₇BrOS

Chemical Property of C₂₁H₂₇BrOS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₂₇BrOS

There total 1 articles about C₂₁H₂₇BrOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

o-bromothiophenol (6320-02-1) + 3,5-di-tert-butyl-2-hydroxybenzyl bromide (194734-57-1) → C21H27BrOS (1392504-20-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/om300505m

Reference yield: 97.0%

C21H27BrOS (1392504-20-9) + trimethylaluminum (75-24-1) → C23H32AlBrOS (1392504-17-4)

Guidance literature:

In benzene; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/om300505m

Reference yield: 78.0%

C21H27BrOS (1392504-20-9) + dibutylmagnesium (1191-47-5) → C25H35BrMgOS

Guidance literature:

In benzene; at 20 ℃; for 2h; Inert atmosphere; Glovebox;

DOI:10.1039/c3dt51219c

upstream raw materials:

o-bromothiophenol

3,5-di-tert-butyl-2-hydroxybenzyl bromide

Downstream raw materials:

C₂₃H₃₂AlBrOS