4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Base Information

Chemical Name:4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin
CAS No.:77016-05-8
Molecular Formula:C₁₉H₃₉N₅O₉
Molecular Weight:481.547
Hs Code.:

Synonyms:4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

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Chemical Property of 4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

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Technology Process of 4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

There total 3 articles about 4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 4-O-(6'-O-Acetyl-2',4'-diazido-3'-O-benzyl-2',4'-didesoxy-α-D-glucopyranosyl)-6-O-<2''-O-acetyl-3''-<(benzyloxycarbonyl)methylamino>-3''-desoxy-4''-C-methyl-β-L-arabinopyranosyl>-1,3-bis-N-(benzyloxycarbonyl)-2-desoxy-D-streptamin

: 77016-05-8
4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; at -60 ℃;

Reference yield:

: 61135-02-2
Acetic acid (2S,3S,4S,5R,6S)-3,5-diazido-4-benzyloxy-6-chloro-tetrahydro-pyran-2-ylmethyl ester

: 77016-05-8
4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Drierite, molecular sieve 4 Angstroem, Hg(CN)2 / 1.) CH₃CN, PhMe, 60 deg C, 2.) PhMe, CH₃CN, reflux

2: 36 percent / Na, NH₃ (liquid) / tetrahydrofuran / -60 °C

With calcium sulfate; 4 A molecular sieve; ammonia; sodium; mercury(II) cyanide; In tetrahydrofuran;

Reference yield:

: 51587-77-0
Acetic acid (2R,3R,4R,5R)-4-(benzyloxycarbonyl-methyl-amino)-2-((1S,2S,3R,4S,6R)-4,6-bis-benzyloxycarbonylamino-2,3-dihydroxy-cyclohexyloxy)-5-hydroxy-5-methyl-tetrahydro-pyran-3-yl ester

: 77016-05-8
4-O-(2',4'-Diamino-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Drierite, molecular sieve 4 Angstroem, Hg(CN)2 / 1.) CH₃CN, PhMe, 60 deg C, 2.) PhMe, CH₃CN, reflux

2: 36 percent / Na, NH₃ (liquid) / tetrahydrofuran / -60 °C

With calcium sulfate; 4 A molecular sieve; ammonia; sodium; mercury(II) cyanide; In tetrahydrofuran;