C₃₄H₂₈N₂O₆S₄

Base Information

Chemical Name:C₃₄H₂₈N₂O₆S₄
CAS No.:1402592-84-0
Molecular Formula:C₃₄H₂₈N₂O₆S₄
Molecular Weight:688.87
Hs Code.:

C<sub>34</sub>H<sub>28</sub>N<sub>2</sub>O<sub>6</sub>S<sub>4</sub>

Synonyms:C₃₄H₂₈N₂O₆S₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₂₈N₂O₆S₄

Chemical Property:

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Technology Process of C₃₄H₂₈N₂O₆S₄

There total 14 articles about C₃₄H₂₈N₂O₆S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 103-82-2
phenylacetic acid

: 1402592-82-8
C₁₈H₁₆N₂O₄S₄

: 1402592-84-0
C₃₄H₂₈N₂O₆S₄

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 25 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ja308429f

Reference yield:

: 144534-57-6
(2S,3aR,7aR)-3a-Hydroxy-6-oxo-2,3,3a,6,7,7a-hexahydro-indole-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

: 1402592-84-0
C₃₄H₂₈N₂O₆S₄

Guidance literature:: Multi-step reaction with 14 steps

1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 4 h / -20 - 0 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

3: palladium diacetate; triethylamine; triphenylphosphine / toluene / 3.33 h / 25 - 110 °C / Inert atmosphere

4: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 24 h / 25 °C / Inert atmosphere; UV-irradiation

5: thiourea / methanol / 2 h / 25 °C / Inert atmosphere

6: triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

7: toluene / 3 h / 110 °C / Inert atmosphere

8: phosphorous acid trimethyl ester / 16 h / 111 °C / Inert atmosphere

9: hydrogenchloride / diethyl ether; dichloromethane / 0.25 h / 0 °C / Inert atmosphere

10: trifluoroacetic acid / dichloromethane / 4 h / 0 - 25 °C / Inert atmosphere

11: N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 0 - 25 °C / Inert atmosphere

12: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diethylamine; 1,4-di(diphenylphosphino)-butane / tetrahydrofuran / 2.05 h / 25 °C / Inert atmosphere

13: sulfur; lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 5 h / 25 °C / Inert atmosphere

14: dmap; dicyclohexyl-carbodiimide / dichloromethane / 5 h / 0 - 25 °C / Inert atmosphere

With hydrogenchloride; sulfur; dmap; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cerium(III) chloride heptahydrate; oxygen; palladium diacetate; 5,15,10,20-tetraphenylporphyrin; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; thiourea; dicyclohexyl-carbodiimide; triphenylphosphine; 1,4-di(diphenylphosphino)-butane; trifluoroacetic acid; lithium hexamethyldisilazane; phosphorous acid trimethyl ester; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 1: |Luche Cerium Reduction;
DOI:10.1021/ja308429f

Reference yield:

: 1402592-61-3
C₁₅H₂₃NO₆

: 1402592-84-0
C₃₄H₂₈N₂O₆S₄

Guidance literature:: Multi-step reaction with 13 steps

1: dmap; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: palladium diacetate; triethylamine; triphenylphosphine / toluene / 3.33 h / 25 - 110 °C / Inert atmosphere

3: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 24 h / 25 °C / Inert atmosphere; UV-irradiation

4: thiourea / methanol / 2 h / 25 °C / Inert atmosphere

5: triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

6: toluene / 3 h / 110 °C / Inert atmosphere

7: phosphorous acid trimethyl ester / 16 h / 111 °C / Inert atmosphere

8: hydrogenchloride / diethyl ether; dichloromethane / 0.25 h / 0 °C / Inert atmosphere

9: trifluoroacetic acid / dichloromethane / 4 h / 0 - 25 °C / Inert atmosphere

10: N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 0 - 25 °C / Inert atmosphere

11: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diethylamine; 1,4-di(diphenylphosphino)-butane / tetrahydrofuran / 2.05 h / 25 °C / Inert atmosphere

12: sulfur; lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 5 h / 25 °C / Inert atmosphere

13: dmap; dicyclohexyl-carbodiimide / dichloromethane / 5 h / 0 - 25 °C / Inert atmosphere

With hydrogenchloride; sulfur; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; oxygen; palladium diacetate; 5,15,10,20-tetraphenylporphyrin; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; thiourea; dicyclohexyl-carbodiimide; triphenylphosphine; 1,4-di(diphenylphosphino)-butane; trifluoroacetic acid; lithium hexamethyldisilazane; phosphorous acid trimethyl ester; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja308429f