Boc-β-OH-Phe-D-Phe-D-Leu-OH

Base Information

Chemical Name:Boc-β-OH-Phe-D-Phe-D-Leu-OH
CAS No.:1357008-28-6
Molecular Formula:C₂₉H₃₉N₃O₇
Molecular Weight:541.645
Hs Code.:

Synonyms:Boc-β-OH-Phe-D-Phe-D-Leu-OH

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Chemical Property of Boc-β-OH-Phe-D-Phe-D-Leu-OH

Chemical Property:

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Technology Process of Boc-β-OH-Phe-D-Phe-D-Leu-OH

There total 1 articles about Boc-β-OH-Phe-D-Phe-D-Leu-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₈N₃O₇Pol

: 1357008-28-6
Boc-β-OH-Phe-D-Phe-D-Leu-OH

Guidance literature:: With 2,2,2-trifluoroethanol; In dichloromethane; at 20 ℃; for 24h; solid phase reaction;
DOI:10.1016/j.tet.2011.11.089

Reference yield: 22.0%

: 1357008-31-1
C₁₀H₁₆N₂O₃

: 1357008-28-6
Boc-β-OH-Phe-D-Phe-D-Leu-OH

: 1357008-32-2
C₃₉H₅₃N₅O₉

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 1357008-28-6
Boc-β-OH-Phe-D-Phe-D-Leu-OH

: 1357008-33-3
C₃₈H₅₁N₅O₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2.1: dihydrogen peroxide; lithium hydroxide / methanol / 3 h / 20 °C

2.2: pH 1

With dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089