Technology Process of C50H32O14
There total 4 articles about C50H32O14 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
N,N-dimethyl-formamide;
for 24h;
Ambient temperature;
DOI:10.1039/a700841d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / 4-N,N-dimethylaminopyridinium toluene-p-sulfonate, DCC / CH2Cl2 / 20 h / Ambient temperature
2: 95 percent / H2 / 5percent Pd/C / tetrahydrofuran / 48 h / Ambient temperature
3: 84.1 percent / 4-N,N-dimethylaminopyridinium toluene-p-sulfonate, DCC / dimethylformamide / 24 h / Ambient temperature
With
hydrogen; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/a700841d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / 4-N,N-dimethylaminopyridinium toluene-p-sulfonate, DCC / CH2Cl2 / 20 h / Ambient temperature
2: 95 percent / H2 / 5percent Pd/C / tetrahydrofuran / 48 h / Ambient temperature
3: 84.1 percent / 4-N,N-dimethylaminopyridinium toluene-p-sulfonate, DCC / dimethylformamide / 24 h / Ambient temperature
With
hydrogen; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/a700841d
