2-[4-(Bromomethyl)phenyl]-1,1,1,3,3,3-hexafluoropropan-2-ol

Base Information

• Chemical Name: 2-[4-(Bromomethyl)phenyl]-1,1,1,3,3,3-hexafluoropropan-2-ol
• CAS No.: 202134-57-4
• Molecular Formula: C10H7 Br F6 O
• Molecular Weight: 337.059
• Hs Code.: 2909309090
• Mol file: 202134-57-4.mol

Synonyms:2-[4-(Bromomethyl)phenyl]-1,1,1,3,3,3-hexafluoropropan-2-ol

Chemical Property of 2-[4-(Bromomethyl)phenyl]-1,1,1,3,3,3-hexafluoropropan-2-ol

Chemical Property:

• Boiling Point: 300.2±42.0 °C(Predicted)
• PKA: 9.10±0.15(Predicted)
• PSA: 20.23000
• Density: 1.690±0.06 g/cm3(Predicted)
• LogP: 3.89370
• Sensitive.: Lachrymatory

Purity/Quality:

99%, ^*data from raw suppliers

2-[4-(Bromomethyl)phenyl]-1,1,1,3,3,3-hexafluoropropan-2-ol ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C,T

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[4-(Bromomethyl)phenyl]-1,1,1,3,3,3-hexafluoropropan-2-ol

There total 2 articles about 2-[4-(Bromomethyl)phenyl]-1,1,1,3,3,3-hexafluoropropan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,1,1,3,3,3-hexafluoro-2-(p-tolyl)propan-2-ol (2010-61-9) → 2-(4-(bromomethyl)phenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol (202134-57-4)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 20 ℃; for 50h; Heating / reflux;

Reference yield:

1,1,1,3,3,3-hexafluoro-2-(p-tolyl)propan-2-ol (2010-61-9) → 2-(4-(bromomethyl)phenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol (202134-57-4) + 2-(4-(dibromomethyl)phenyl)- 1,1,1,3,3,3-hexafluoropropan-2-ol

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 80 ℃; for 2h;

Reference yield: 52.0%

2-(4-(bromomethyl)phenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol (202134-57-4) + thiophenol (108-98-5) → 1,1,1,3,3,3-hexafluoro-2-(4-((phenylsulfonyl)methyl)phenyl)propan-2-ol

Guidance literature:

2-(4-(bromomethyl)phenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol; thiophenol; With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 18h;

With PS-trisamine resin; In tetrahydrofuran; for 18h;

With Oxone; sodium hydrogencarbonate; more than 3 stages;

upstream raw materials:

1,1,1,3,3,3-hexafluoro-2-(p-tolyl)propan-2-ol

Downstream raw materials:

[4-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-phenyl]-acetonitrile

4-methyl-3-oxo-2-[4-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-phenyl]-pentanenitrile

3-oxo-2-[4-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-phenyl]-pentanenitrile

3-furan-3-yl-3-oxo-2-[4-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-phenyl]-propionitrile

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