N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

Base Information

Chemical Name:N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide
CAS No.:505077-55-4
Molecular Formula:C₃₃H₄₅NO₈SSi
Molecular Weight:643.874
Hs Code.:

Synonyms:N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

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Chemical Property of N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

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Technology Process of N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

There total 7 articles about N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 217642-64-3
N-[2-(2-O-acetyl-3-O-allyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

: 505077-55-4
N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

Guidance literature:: With potassium diazodicarboxylate; acetic acid; In acetonitrile; at 0 ℃; for 2h;
DOI:10.1016/S0008-6215(02)00301-4

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 505077-55-4
N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / imidazole; DMAP / CH₂Cl₂ / 2 h / 20 °C

2: 98 percent / potassium azodicarboxylate; HOAc / acetonitrile / 2 h / 0 °C

With 1H-imidazole; dmap; potassium diazodicarboxylate; acetic acid; In dichloromethane; acetonitrile;
DOI:10.1016/S0008-6215(02)00301-4

Reference yield:

: 163924-98-9
Succinic acid methyl ester monocysteamide

: 505077-55-4
N-[2-(2'-O-acetyl-6'-O-tert-butyldiphenylsilyl-3'-O-propyl-β-D-glucopyranosylsulfanyl)ethyl]succinimide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / BF₃*OEt₂ / CH₂Cl₂ / 6 h / 0 - 25 °C

2: 90 percent / NaOMe / methanol / 6 h / 0 °C

3: 90 percent / imidazole; DMAP / CH₂Cl₂ / 2 h / 20 °C

4: 98 percent / potassium azodicarboxylate; HOAc / acetonitrile / 2 h / 0 °C

With 1H-imidazole; dmap; boron trifluoride diethyl etherate; sodium methylate; potassium diazodicarboxylate; acetic acid; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0008-6215(02)00301-4