C₂₉H₄₈O₅Si

Base Information

Chemical Name:C₂₉H₄₈O₅Si
CAS No.:1252651-66-3
Molecular Formula:C₂₉H₄₈O₅Si
Molecular Weight:504.783
Hs Code.:

C<sub>29</sub>H<sub>48</sub>O<sub>5</sub>Si

Synonyms:C₂₉H₄₈O₅Si

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Chemical Property of C₂₉H₄₈O₅Si

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Technology Process of C₂₉H₄₈O₅Si

There total 11 articles about C₂₉H₄₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1252651-59-4
C₂₈H₄₆O₆Si

: 917-54-4
methyllithium

: 1252651-66-3
C₂₉H₄₈O₅Si

Guidance literature:: C₂₈H₄₆O₆Si; With isopropylmagnesium chloride; N,O-dimethylhydroxylamine*hydrochloride; In tetrahydrofuran; at -15 - 20 ℃; Inert atmosphere;

methyllithium; In tetrahydrofuran; diethyl ether; at -78 - 0 ℃; Inert atmosphere;

With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja107190w

Reference yield:

: C₃₁H₅₇NO₇Si

: 1252651-66-3
C₂₉H₄₈O₅Si

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja2041964

Reference yield:

: 1252651-59-4
C₂₈H₄₆O₆Si

: 1252651-66-3
C₂₉H₄₈O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: tetrahydrofuran; diethyl ether / -78 - 0 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

With isopropylmagnesium chloride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja2041964