2--2-methylpropanedioic acid, dimethyl ester

Base Information

Chemical Name:2--2-methylpropanedioic acid, dimethyl ester
CAS No.:129152-00-7
Molecular Formula:C₁₄H₁₇BrO₅
Molecular Weight:345.19
Hs Code.:

2-<bromo(4-methoxyphenyl)methyl>-2-methylpropanedioic acid, dimethyl ester

Synonyms:2--2-methylpropanedioic acid, dimethyl ester

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Chemical Property of 2--2-methylpropanedioic acid, dimethyl ester

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Technology Process of 2--2-methylpropanedioic acid, dimethyl ester

There total 3 articles about 2--2-methylpropanedioic acid, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 21118-89-8
2-<(4-methoxyphenyl)methyl>-2-methylpropanedioic acid, dimethyl ester

: 129152-00-7
2--2-methylpropanedioic acid, dimethyl ester

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 3h; Irradiation;
DOI:10.1021/jo00308a013

Reference yield:

: 609-02-9
methyl-malonic acid dimethylester

: 129152-00-7
2--2-methylpropanedioic acid, dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1) mineral oil, DMF, 40 min, 2.) 4 h

2: 87 percent / N-bromosuccinimide, azobis(isobutrylnitrile) / CCl₄ / 3 h / Irradiation

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrachloromethane;
DOI:10.1021/jo00308a013

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 129152-00-7
2--2-methylpropanedioic acid, dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1) mineral oil, DMF, 40 min, 2.) 4 h

2: 87 percent / N-bromosuccinimide, azobis(isobutrylnitrile) / CCl₄ / 3 h / Irradiation

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrachloromethane;
DOI:10.1021/jo00308a013