4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester

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Chemical Name:4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester
CAS No.:857887-62-8
Molecular Formula:C₂₇H₃₀N₂O₉S
Molecular Weight:558.609
Hs Code.:

Synonyms:4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester

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Chemical Property of 4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester

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Technology Process of 4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester

There total 3 articles about 4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 857887-61-7
(S)-2-(2-(2-methoxyethoxy)ethoxy)propan-1-ol

: 857887-60-6
4-(2-nitro-benzenesulfonylamino)-benzoic acid phenyl ester

: 857887-62-8
4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 15h;
DOI:10.1021/ja0455291

Reference yield:

: 10268-70-9
phenyl p-aminobenzoate

: 857887-62-8
4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine / 2 h / 20 °C

2: 67 percent / diethyl azodicarboxylate; PPh₃ / tetrahydrofuran / 15 h / 20 °C

With pyridine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2: Mitsunobu reaction;
DOI:10.1021/ja0455291

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 857887-62-8
4-[{(S)-2-[2-(2-Methoxy-ethoxy)-ethoxy]-propyl}-(2-nitro-benzenesulfonyl)-amino]-benzoic acid phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine / 2 h / 20 °C

2: 67 percent / diethyl azodicarboxylate; PPh₃ / tetrahydrofuran / 15 h / 20 °C

With pyridine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2: Mitsunobu reaction;
DOI:10.1021/ja0455291