(4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

Base Information

Chemical Name:(4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone
CAS No.:950479-13-7
Molecular Formula:C₂₆H₃₃NO₆
Molecular Weight:455.551
Hs Code.:

Synonyms:(4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

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Chemical Property of (4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

Chemical Property:

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Technology Process of (4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

There total 1 articles about (4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: (2S,3R)-3-(4-methxoybenzyloxy)-2-mehtylpentanal

: 110905-24-3
(4R)-3-(bromoacetyl)-4-(phenylmethyl)-2-oxazolidinone

: 950479-13-7
(4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

: (4R,3'R,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1002/ejoc.200700254

Reference yield: 82.0%

: 950479-13-7
(4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

: 69739-34-0
t-butyldimethylsiyl triflate

: 950479-16-0
C₃₂H₄₇NO₆Si

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/ejoc.200700254

Reference yield:

: 950479-13-7
(4R,3'S,4'R,5'R)-4-benzyl-[5'-[(4-methoxybenzyl)oxy]-3'-hydroxy-4'-methylheptnaoyl]-2-oxazolidinone

: 950479-17-1
C₂₂H₄₀O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

2: 94 percent / lithium borohydride / diethyl ether; H₂O; tetrahydrofuran / 1.17 h / 0 - 20 °C

With 2,6-dimethylpyridine; lithium borohydride; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1002/ejoc.200700254