(4S,5S)-4,8-Bis-(3,5-bis-trifluoromethyl-phenyl)-2,10-di-tert-butyl-6-(2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-3,9-dimethoxy-5H-dibenzo[c,e]azepinium tetraphenylborate

Base Information

• Chemical Name: (4S,5S)-4,8-Bis-(3,5-bis-trifluoromethyl-phenyl)-2,10-di-tert-butyl-6-(2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-3,9-dimethoxy-5H-dibenzo[c,e]azepinium tetraphenylborate
• CAS No.: 1417576-98-7
• Molecular Formula: C₂₄H₂₀B*C₅₂H₅₀F₁₂NO₄
• Molecular Weight: 1300.19
• Mol file: 1417576-98-7.mol

Synonyms:(4S,5S)-4,8-Bis-(3,5-bis-trifluoromethyl-phenyl)-2,10-di-tert-butyl-6-(2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-3,9-dimethoxy-5H-dibenzo[c,e]azepinium tetraphenylborate

Chemical Property of (4S,5S)-4,8-Bis-(3,5-bis-trifluoromethyl-phenyl)-2,10-di-tert-butyl-6-(2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-3,9-dimethoxy-5H-dibenzo[c,e]azepinium tetraphenylborate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (4S,5S)-4,8-Bis-(3,5-bis-trifluoromethyl-phenyl)-2,10-di-tert-butyl-6-(2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-3,9-dimethoxy-5H-dibenzo[c,e]azepinium tetraphenylborate

There total 1 articles about (4S,5S)-4,8-Bis-(3,5-bis-trifluoromethyl-phenyl)-2,10-di-tert-butyl-6-(2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-3,9-dimethoxy-5H-dibenzo[c,e]azepinium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-(4S,5S)-5-(2,2-Dimethyl-4-phenyl-1,3-dioxanyl)-3,3'-bis-(3,5-(trifluoromethyl)-phenyl)-5,5'-di-tert-butyl-4,4'-dimethoxy-2,7-dihydrodibenzo[c,e]azepine (1417577-00-4) + sodium tetraphenyl borate (143-66-8) → (4S,5S)-4,8-Bis-(3,5-bis-trifluoromethyl-phenyl)-2,10-di-tert-butyl-6-(2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-3,9-dimethoxy-5H-dibenzo[c,e]azepinium tetraphenylborate (1417576-98-7)

Guidance literature:

N-(4S,5S)-5-(2,2-Dimethyl-4-phenyl-1,3-dioxanyl)-3,3'-bis-(3,5-(trifluoromethyl)-phenyl)-5,5'-di-tert-butyl-4,4'-dimethoxy-2,7-dihydrodibenzo[c,e]azepine; With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 20 ℃; for 3h; Reflux;

sodium tetraphenyl borate; In ethanol; acetonitrile; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.tet.2012.10.076

upstream raw materials:

N-(4S,5S)-5-(2,2-Dimethyl-4-phenyl-1,3-dioxanyl)-3,3'-bis-(3,5-(trifluoromethyl)-phenyl)-5,5'-di-tert-butyl-4,4'-dimethoxy-2,7-dihydrodibenzo[c,e]azepine

sodium tetraphenyl borate