Technology Process of C28H30N8O6
There total 5 articles about C28H30N8O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C31H34N8O6;
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 60 ℃;
for 24h;
With
potassium carbonate;
In
tetrahydrofuran; water;
pH=10;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trichlorophosphate / pyridine / 24 h / 0 - 20 °C / Inert atmosphere
2.1: piperidine / dichloromethane / 0.17 h / 20 °C
2.2: 0.17 h / 20 °C
3.1: sodium tetrahydroborate / isopropyl alcohol; water / 1 h / 60 °C
3.2: 48 h / 20 - 80 °C
4.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere
5.1: hydrogenchloride / water; tetrahydrofuran / 24 h / 60 °C
5.2: pH 10
With
piperidine; hydrogenchloride; sodium tetrahydroborate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; trichlorophosphate;
In
tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
1.1: Vilsmeier Formylation / 2.1: Knoevenagel Condensation;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere
2.1: hydrogenchloride / water; tetrahydrofuran / 24 h / 60 °C
2.2: pH 10
With
hydrogenchloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;