5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate

Base Information

Chemical Name:5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate
CAS No.:148492-44-8
Molecular Formula:C₂₂H₂₀N₆S₄
Molecular Weight:496.705
Hs Code.:

Synonyms:5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate

Chemical Property:

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Technology Process of 5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate

There total 1 articles about 5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 31728-63-9
5-imino-3-methyl-1-phenyl-Δ²-pyrazolin-4-dithiocarbamic acid

: 148492-44-8
5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate

Guidance literature:: With trichlorophosphate; In chloroform; at 50 ℃; for 2h;

Reference yield:

: 148492-44-8
5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate

: 4-<3'-(5''-amino-4''-pyrazolyl)-3-methyl-1,1'-diphenyl-1'H-pyrazole-4'-dithiocarbamate-2-pyrazoline>dithiocarbamate-5,5'-dione

Guidance literature:: Multi-step reaction with 4 steps

1: POCl₃

2: 70 percent / NH₂OH*HCl / ethanol / 3 h / Heating

3: 63 percent / 5percent aq. NaOH / 45 - 50 °C

4: 60 percent / N₂H₄*H₂O / acetic acid / 3 h / Heating

With sodium hydroxide; hydroxylamine hydrochloride; hydrazine hydrate; trichlorophosphate; In ethanol; acetic acid;

Reference yield:

: 148492-44-8
5,5'-diimino-3,3'-dimethyl-1,1'-diphenyl-bi-4H-pyrazole-4,4'-dithiocarbamate

: 4-<5'-imino-3'-(1''-formyl-2''-piperidinylethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃

2: 78 percent / ethanol / 0.67 h / Heating

With trichlorophosphate; In ethanol;