2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester

Base Information

• Chemical Name: 2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester
• CAS No.: 214853-58-4
• Molecular Formula: C₁₇H₃₀O₂
• Molecular Weight: 266.424
• Mol file: 214853-58-4.mol

Synonyms:2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester

Chemical Property of 2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester

There total 3 articles about 2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,2-dimethylpent-4-enoyl chloride (39482-46-7) + 4-(1,1-dimethylethyl)-cyclohexanol (98-52-2) → 2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester (214853-58-4)

Guidance literature:

With triethylamine; In dichloromethane; at 25 ℃; for 15h;

DOI:10.1016/S0040-4039(98)01465-8

Reference yield:

2,2-dimethylpent-4-enoic acid (16386-93-9) → 2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester (214853-58-4)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / benzene / 15 h / 80 °C

2: 88 percent / triethylamine / CH₂Cl₂ / 15 h / 25 °C

With thionyl chloride; triethylamine; In dichloromethane; benzene;

DOI:10.1016/S0040-4039(98)01465-8

Reference yield:

methyl 2,2-dimethyl-4-pentenoate (76352-72-2) → 2,2-Dimethyl-pent-4-enoic acid 4-tert-butyl-cyclohexyl ester (214853-58-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 99 percent / NaOH / methanol; H₂O / 80 °C

2: thionyl chloride / benzene / 15 h / 80 °C

3: 88 percent / triethylamine / CH₂Cl₂ / 15 h / 25 °C

With sodium hydroxide; thionyl chloride; triethylamine; In methanol; dichloromethane; water; benzene;

DOI:10.1016/S0040-4039(98)01465-8

upstream raw materials:

2,2-dimethylpent-4-enoyl chloride

4-(1,1-dimethylethyl)-cyclohexanol

2,2-dimethylpent-4-enoic acid

methyl 2,2-dimethyl-4-pentenoate

Downstream raw materials:

4-(1,1-dimethylethyl)-cyclohexanol