(2,4,6-Me₃C₆H₂)SbH₂

Base Information

Chemical Name:(2,4,6-Me₃C₆H₂)SbH₂
CAS No.:875587-31-8
Molecular Formula:C₉H₁₃Sb
Molecular Weight:242.952
Hs Code.:

(2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)SbH<sub>2</sub>

Synonyms:(2,4,6-Me₃C₆H₂)SbH₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,4,6-Me₃C₆H₂)SbH₂

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Technology Process of (2,4,6-Me₃C₆H₂)SbH₂

There total 1 articles about (2,4,6-Me₃C₆H₂)SbH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 16853-85-3
lithium aluminium tetrahydride

: 106870-56-8
mesitylantimony dichloride

: 875587-31-8
(2,4,6-Me₃C₆H₂)SbH₂

Guidance literature:: In diethyl ether; all manipulations under Ar atm.; soln. of Sb compd. added dropwise to cold (-80°C) Li compd., warmed to -10°C; filtered through cooled frit, solvent removed in vac. at -10°C;
DOI:10.1002/zaac.200400497

Reference yield: 99.0%

: (η5-C5H5)(η5-C5Me5)HfHCl

: 875587-31-8
(2,4,6-Me₃C₆H₂)SbH₂

: [(cyclopentadienyl)(pentamethylcyclopentadienyl)HfCl(Sb(H)(mesityl))]

Guidance literature:: In benzene-d6; byproducts: H2; by addn. of Sb-contg. compd. (1 equiv.) to a soln. of Zr-contg. compd. in C6D6; fast σ-bond metathesis: t(1/2) < 2 min; detd. by (1)H and (13)C NMR spectra studies;
DOI:10.1002/anie.200600318

Reference yield: 95.0%

: 875587-31-8
(2,4,6-Me₃C₆H₂)SbH₂

: 106870-65-9,118456-82-9
(MesSb)4

Guidance literature:: Schwartz's reagent; In benzene-d6; byproducts: H2; by a react. of Sb-contg. compd. (20 equiv.) with Zr-contg. compd. at 25°C for < 0.5 h; according to M. Ates et al. Z. Naturforsch. B 1986, 41, 321-326;
DOI:10.1002/anie.200600318