9,10-Diazapentacyclo<4.4.0.0^2,4.0^3,8.0^5,7>decan-9,10-dicarbonsaeurediphenylester

Base Information

• Chemical Name: 9,10-Diazapentacyclo<4.4.0.0^2,4.0^3,8.0^5,7>decan-9,10-dicarbonsaeurediphenylester
• CAS No.: 142320-89-6
• Molecular Formula: C₂₂H₁₈N₂O₄
• Molecular Weight: 374.396
• Mol file: 142320-89-6.mol

Synonyms:9,10-Diazapentacyclo<4.4.0.0^2,4.0^3,8.0^5,7>decan-9,10-dicarbonsaeurediphenylester

Chemical Property of 9,10-Diazapentacyclo<4.4.0.0^2,4.0^3,8.0^5,7>decan-9,10-dicarbonsaeurediphenylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,10-Diazapentacyclo<4.4.0.0^2,4.0^3,8.0^5,7>decan-9,10-dicarbonsaeurediphenylester

There total 1 articles about 9,10-Diazapentacyclo<4.4.0.0^2,4.0^3,8.0^5,7>decan-9,10-dicarbonsaeurediphenylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

9,10-Diazapentacyclo<4.4.0.02,5.03,8.04,7>decan-9,10-dicarbonsaeure-diphenylester (81226-17-7) → 9,10-Diazapentacyclo<4.4.0.02,4.03,8.05,7>decan-9,10-dicarbonsaeurediphenylester (142320-89-6)

Guidance literature:

With silver nitrate; In methanol; for 144h; Heating;

Reference yield: 72.0%

9,10-Diazapentacyclo<4.4.0.02,4.03,8.05,7>decan-9,10-dicarbonsaeurediphenylester (142320-89-6) → (+/-)-5,6-Diazatricyclo<5.3.0.04,8>deca-2,9-dien-5,6-dicarbonsaeurediphenylester (89757-44-8,89757-46-0,89757-47-1)

Guidance literature:

With trifluoroacetic acid; for 1.5h; Ambient temperature;

Reference yield:

9,10-Diazapentacyclo<4.4.0.02,4.03,8.05,7>decan-9,10-dicarbonsaeurediphenylester (142320-89-6) → (+/-)-5,6-Diazatricyclo<5.3.0.04,8>dec-2-en-5,6-dicarbonsaeure-diphenylester (89757-45-9,142433-83-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / trifluoroacetic acid / 1.5 h / Ambient temperature

2: 90 percent / H₂ / Pd-CaCO₃ / ethyl acetate / Ambient temperature

With hydrogen; trifluoroacetic acid; Lindlar's catalyst; In ethyl acetate;

upstream raw materials:

9,10-Diazapentacyclo<4.4.0.0^2,5.0^3,8.0^4,7>decan-9,10-dicarbonsaeure-diphenylester

Downstream raw materials:

(+/-)-5,6-Diazatricyclo<5.3.0.0^4,8>deca-2,9-dien-5,6-dicarbonsaeurediphenylester

(+/-)-5,6-Diazatricyclo<5.3.0.0^4,8>dec-2-en-5,6-dicarbonsaeure-diphenylester

(+/-)-5,6-Diazatricyclo<5.3.0.0^4,8>decan-5,6-dicarbonsaeure-diphenylester