(R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate

Base Information

Chemical Name:(R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate
CAS No.:916985-11-0
Molecular Formula:C₂₂H₂₅FN₄O₂
Molecular Weight:396.465
Hs Code.:

Synonyms:(R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate

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Chemical Property of (R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate

Chemical Property:

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Technology Process of (R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate

There total 4 articles about (R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-fluoro-benzenecarboximidothioic acid methyl ester

: 916985-10-9
(2R)-N-amino-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

: 916985-11-0
(R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; at 0 - 80 ℃; for 5h;

Reference yield:

: 1194-02-1,143234-87-1
4-fluorobenzonitrile

: 916985-11-0
(R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: O,O-Diethyl hydrogen phosphorodithioate / tetrahydrofuran; water / 8 h / 80 °C

2: acetonitrile / 1 h / 80 °C

3: N-ethyl-N,N-diisopropylamine / ethanol / 5 h / 80 °C

With O,O-Diethyl hydrogen phosphorodithioate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; water; acetonitrile;

Reference yield:

: 240420-27-3
methyl (2R)-2-[(tert-butoxycarbonyl)amino]-4-phenylbutanoate

: 916985-11-0
(R)-tert-butyl 1-(3-(4-fluorophenyl)-1H-1,2,4-triazol-5-yl)-3-phenylpropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / 3 h / 80 °C

2: N-ethyl-N,N-diisopropylamine / ethanol / 5 h / 80 °C

With hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In ethanol;