6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

Base Information

Chemical Name:6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose
CAS No.:58475-19-7
Molecular Formula:C₁₆H₂₂O₇S
Molecular Weight:358.412
Hs Code.:

Synonyms:6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

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Chemical Property of 6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

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Technology Process of 6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

There total 6 articles about 6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41341-67-7
3-O-Benzyl-6-desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

: 58475-19-7
6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 40 ℃; for 7h; Yield given;

Reference yield:

: 18439-45-7,70632-45-0,87938-30-5,18439-44-6
3-O-Benzyl-6-desoxy-1,2-O-isopropyliden-α-D-gluco-hexofuranose

: 58475-19-7
6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine / pyridine / 72 h / Ambient temperature

2: H₂ / Pd/C / ethanol / 7 h / 40 °C

With dmap; hydrogen; palladium on activated charcoal; In pyridine; ethanol;

Reference yield:

: 23313-03-3
(R)-2-[(3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]-2-hydroxyethyl 4-methylbenzenesulfonate

: 58475-19-7
6-Desoxy-1,2-O-isopropyliden-5-O-(p-tolylsulfonyl)-α-D-gluco-hexofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / LiAlH₄ / diethyl ether / 1.) reflux, 3 h; 2.) room temp., 15 h

2: 4-(dimethylamino)pyridine / pyridine / 72 h / Ambient temperature

3: H₂ / Pd/C / ethanol / 7 h / 40 °C

With dmap; lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In pyridine; diethyl ether; ethanol;