C₁₆H₁₇F₃INS

Base Information

• Chemical Name: C₁₆H₁₇F₃INS
• CAS No.: 1373155-52-2
• Molecular Formula: C₁₆H₁₇F₃INS
• Molecular Weight: 439.283
• Mol file: 1373155-52-2.mol

Synonyms:C₁₆H₁₇F₃INS

Chemical Property of C₁₆H₁₇F₃INS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₇F₃INS

There total 1 articles about C₁₆H₁₇F₃INS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

S-methyl tetrahydro thiophenium iodide (28608-92-6) + 4-trifluoroacetyl-3-methyl-2-phenyl-1,3-oxazol-3-ium-5-olate (14119-99-4) → 4-trifluoromethyl-1-methyl-2-phenyl-1H-pyrrole (1253394-12-5) + C16H17F3INS (1373155-52-2)

Guidance literature:

S-methyl tetrahydro thiophenium iodide; With n-butyllithium; In tetrahydrofuran; at -20 ℃; for 0.333333h; Inert atmosphere;

4-trifluoroacetyl-3-methyl-2-phenyl-1,3-oxazol-3-ium-5-olate; In tetrahydrofuran; at -20 - 20 ℃;

With acetic acid; In tetrahydrofuran; at 80 ℃; for 10h; regiospecific reaction;

DOI:10.1016/j.tetlet.2012.03.130

upstream raw materials:

S-methyl tetrahydro thiophenium iodide

4-trifluoroacetyl-3-methyl-2-phenyl-1,3-oxazol-3-ium-5-olate