tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate

Base Information

Chemical Name:tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate
CAS No.:1469268-19-6
Molecular Formula:C₂₇H₃₇N₃O₈
Molecular Weight:531.606
Hs Code.:

Synonyms:tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate

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Chemical Property of tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate

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Technology Process of tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate

There total 6 articles about tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.4%

: 1198475-78-3
(2-{2-[2-(2-chloroacetylamino)-ethoxy]ethoxy}ethyl)carbamic acid tert-butyl ester

: 3743-69-9
N-(2-hydroxyphenyl)-2-phenoxyacetamide

: 1469268-19-6
tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate

Guidance literature:: With potassium carbonate; caesium carbonate; potassium iodide; In acetone; at 60 ℃; for 36h; Inert atmosphere;
DOI:10.1002/anie.201304987

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1469268-19-6
tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 24 h / -20 - 20 °C / Inert atmosphere

3: potassium carbonate; potassium iodide; caesium carbonate / acetone / 36 h / 60 °C / Inert atmosphere

With potassium carbonate; caesium carbonate; triethylamine; potassium iodide; In methanol; dichloromethane; acetone;
DOI:10.1002/anie.201304987

Reference yield:

: 929-59-9,892154-56-2
3,6-dioxa-1,8-diaminooctane

: 1469268-19-6
tert-butyl 2-[2-(2-{2-[2-(2-phenoxyacetamido)phenoxy]acetamido}ethoxy)ethoxy]ethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 24 h / -20 - 20 °C / Inert atmosphere

3: potassium carbonate; potassium iodide; caesium carbonate / acetone / 36 h / 60 °C / Inert atmosphere

With potassium carbonate; caesium carbonate; triethylamine; potassium iodide; In methanol; dichloromethane; acetone;
DOI:10.1002/anie.201304987