5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide

Base Information

Chemical Name:5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide
CAS No.:120344-62-9
Molecular Formula:Br*C₁₇H₁₄N₃S₂
Molecular Weight:404.354
Hs Code.:

Synonyms:5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide

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Technology Process of 5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide

There total 2 articles about 5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 120344-58-3
3-Amino-2-benzylthio-4-phenylthiazolium bromide

: 622-59-3
1-isothiocyanato-4-methylbenzene

: 120344-62-9
5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide

Guidance literature:: With triethylamine; In acetonitrile; for 24h; Ambient temperature;
DOI:10.1055/s-1988-27691

Reference yield:

: 5316-81-4
3-amino-4-phenylthiazoline-2(3H)-thione

: 120344-62-9
5-Phenyl-2-p-tolylamino-thiazolo[2,3-b][1,3,4]thiadiazol-4-ylium; bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: 41 percent / Et₃N / acetonitrile / 24 h / Ambient temperature

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.1055/s-1988-27691