<2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide

Base Information

• Chemical Name: <2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide
• CAS No.: 120423-63-4
• Molecular Formula: C₃₈H₃₄N₄O₄S₄
• Molecular Weight: 738.976

Synonyms:<2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide

Chemical Property of <2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide

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Technology Process of <2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide

There total 6 articles about <2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-bromomethyl-4-phenyl-5-oxo-1,2,6,7,8,9-hexahydrobenzothieno<3,2-e>thiazolo<3,2-a>pyrimidinium tribromide → <2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide (120423-63-4)

Guidance literature:

With water; sodium carbonate; In dimethyl sulfoxide; at 20 ℃; for 0.166667h;

DOI:10.1007/s00044-011-9748-4

Reference yield:

1-Iodomethyl-4-phenyl-1,2,3a,4,6,7,8,9-octahydro-3,10-dithia-4,10b-diaza-cyclopenta[a]fluoren-5-one; compound with GENERIC INORGANIC NEUTRAL COMPONENT → <2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide (120423-63-4)

Guidance literature:

With sodium acetate; In dimethyl sulfoxide; at 25 ℃;

Reference yield:

1-iodomethyl-4-phenyl-5-oxo-1,2,6,7,8,9-hexahydrobenzothieno<3,2-e>thiazolo<3,2-a>pyrimidinium triiodide → <2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide (120423-63-4)

Guidance literature:

With sodium acetate; In water; dimethyl sulfoxide; Yield given;

DOI:10.1007/BF00472400

upstream raw materials:

3-phenyl-2-thio-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

2-mercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine sodium salt

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