1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline

Base Information

• Chemical Name: 1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline
• CAS No.: 100417-01-4
• Molecular Formula: C₂₀H₂₅NO₅
• Molecular Weight: 359.422

Synonyms:1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline

Chemical Property of 1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline

There total 2 articles about 1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-(6,7-Dimethoxy-3,4-dihydro-isoquinolin-1-yl)-heptanedioic acid diethyl ester → 1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline (100417-01-4)

Guidance literature:

With sodium methylate; In toluene; for 9h; Heating;

Reference yield:

→ 1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline (100417-01-4)

Guidance literature:

Reference yield: 88.0%

1-[(3'-ethoxycarbonyl-4'-oxo)-1-cyclohexyl]-3,4-dihydro-6,7-dimethoxyisoquinoline (100417-01-4) → 1-<(3'-methoxycarbonyl-4'-imino)-1'-cyclohexyl>-6,7-dimethoxy-3,4-dihydroisoquinole

Guidance literature:

With ammonia; for 72h; Ambient temperature;

Downstream raw materials:

1-(4'-oxo-1'-cyclohexyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

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