3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide

Base Information

Chemical Name:3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide
CAS No.:1474041-97-8
Molecular Formula:BrH*C₁₆H₂₁ClN₂Se
Molecular Weight:436.681
Hs Code.:

Synonyms:3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide

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Chemical Property of 3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide

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Technology Process of 3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide

There total 3 articles about 3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1474041-89-8
1-(3-chloro-4-methylphenyl)-3-(2-cyclohex-1-enylethyl)selenourea

: 1474041-97-8
3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide

Guidance literature:: With hydrogen bromide; In water; at 100 ℃; for 5h; Reflux;
DOI:10.1134/S0012500813080028

Reference yield:

: 1028862-12-5
C₈H₆ClNSe

: 1474041-97-8
3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 20 °C

2: hydrogen bromide / 5 h / Reflux

With hydrogen bromide; In diethyl ether;
DOI:10.1007/s11172-013-0021-5

Reference yield:

: 6312-80-7
N-(3-chloro-4-methylphenyl)formamide

: 1474041-97-8
3-chloro-4-methylphenyl(1-selena-3-azaspiro[5.5]undec-2-en-2yl)amine hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: phosgene; selenium; triethylamine / toluene / Reflux

2: diethyl ether / 20 °C

3: hydrogen bromide / 5 h / Reflux

With phosgene; selenium; hydrogen bromide; triethylamine; In diethyl ether; toluene;
DOI:10.1007/s11172-013-0021-5