methyl N^α-(N-benzyloxycarbonyl-D-isoglutamyl α-methyl ester)-N^ε-(tert-butyloxycarbonyl)-L-lysinate

Base Information

• Chemical Name: methyl N^α-(N-benzyloxycarbonyl-D-isoglutamyl α-methyl ester)-N^ε-(tert-butyloxycarbonyl)-L-lysinate
• CAS No.: 478920-21-7
• Molecular Formula: C₂₆H₃₉N₃O₉
• Molecular Weight: 537.61

Synonyms:methyl N^α-(N-benzyloxycarbonyl-D-isoglutamyl α-methyl ester)-N^ε-(tert-butyloxycarbonyl)-L-lysinate

Chemical Property of methyl N^α-(N-benzyloxycarbonyl-D-isoglutamyl α-methyl ester)-N^ε-(tert-butyloxycarbonyl)-L-lysinate

Chemical Property:

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Technology Process of methyl N^α-(N-benzyloxycarbonyl-D-isoglutamyl α-methyl ester)-N^ε-(tert-butyloxycarbonyl)-L-lysinate

There total 1 articles about methyl N^α-(N-benzyloxycarbonyl-D-isoglutamyl α-methyl ester)-N^ε-(tert-butyloxycarbonyl)-L-lysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride (2389-48-2) + N-(benzyloxycarbonyl)-D-glutamic acid 1-methyl ester (26566-11-0) → methyl Nα-(N-benzyloxycarbonyl-D-isoglutamyl α-methyl ester)-Nε-(tert-butyloxycarbonyl)-L-lysinate (478920-21-7)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; pH=9 - 9.5;

DOI:10.1002/1099-0690(200208)2002:16<2710::AID-EJOC2710>3.0.CO;2-8

upstream raw materials:

N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride

N-(benzyloxycarbonyl)-D-glutamic acid 1-methyl ester

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