3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene

Base Information

• Chemical Name: 3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene
• CAS No.: 1189561-93-0
• Molecular Formula: C₆₂H₆₂
• Molecular Weight: 807.174

Synonyms:3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene

Chemical Property of 3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene

Chemical Property:

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Technology Process of 3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene

There total 1 articles about 3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diiododibenzo[a,h]anthracene (1189561-88-3) + phenylboronic acid (98-80-6) → 3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene (1189561-93-0)

Guidance literature:

With 1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate; sodium hydroxide; In 1,4-dioxane; water; at 105 ℃; for 6h;

DOI:10.1021/jo9015437

Reference yield: 59.0%

3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene (1189561-93-0) → 2,11-di(tert-butyl)-9,18-di[4-(tert-butyl)phenyl]-dibenzo[a,m]rubicene (1189561-95-2)

Guidance literature:

With ferric(III) bromide; In nitromethane; dichloromethane; at 23 ℃; for 0.5h;

DOI:10.1021/jo9015437

Reference yield: 31.0%

3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diphenyldibenzo[a,h]anthracene (1189561-93-0) → 2,11-di(tert-butyl)-9,18-di[4-(tert-butyl)phenyl]-dibenzo[a,m]rubicene (1189561-95-2) + C62H56Cl2 (1189561-99-6)

Guidance literature:

With iron(III) chloride; In nitromethane; at 23 ℃; for 0.166667h;

DOI:10.1021/jo9015437

upstream raw materials:

3,10-di(tert-butyl)-5,12-di[4-(tert-butyl)phenyl]-6,13-diiododibenzo[a,h]anthracene

phenylboronic acid

Downstream raw materials:

2,11-di(tert-butyl)-9,18-di[4-(tert-butyl)phenyl]-dibenzo[a,m]rubicene

C₆₂H₅₆Cl₂

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