7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one

Base Information

Chemical Name:7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one
CAS No.:1607831-12-8
Molecular Formula:C₁₁H₆Cl₂N₄OS
Molecular Weight:313.167
Hs Code.:

Synonyms:7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one

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Chemical Property of 7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one

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Technology Process of 7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one

There total 4 articles about 7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1607840-38-9
C₁₃H₁₂Cl₂N₄O₂S

: 1607831-12-8
7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one

Guidance literature:: With sodium hydroxide; In ethanol; water; at 100 ℃; for 0.333333h;
DOI:10.1016/j.ejmech.2014.03.063

Reference yield:

: 4640-68-0
3,4-dichlorobenzoyl acetonitrile

: 1607831-12-8
7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / methanol / 1 h / 140 °C / Microwave irradiation

2: N,N-dimethyl-formamide / 5 h / 20 °C

3: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With hydrazine hydrate; sodium hydroxide; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.063

Reference yield:

: 208519-10-2
C₉H₇Cl₂N₃

: 1607831-12-8
7-(3,4-dichloro-phenyl)-2-thioxo-2,3-dihydro-1H-pyrazolo[1,5-a][1,3,5]triazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 5 h / 20 °C

2: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.063