9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine

Base Information

Chemical Name:9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine
CAS No.:86527-22-2
Molecular Formula:C₃₂H₂₃N₇O₁₃S
Molecular Weight:745.64
Hs Code.:

Synonyms:9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine

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Chemical Property of 9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine

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Technology Process of 9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine

There total 3 articles about 9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 86527-21-1
9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-chloropurine

: 86527-22-2
9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine

Guidance literature:: With thiourea; In ethanol; for 6h; Heating;
DOI:10.1021/jm00364a032

Reference yield:

: 32865-86-4
6-chloro-9-trimethylsilylpurine

: 86527-22-2
9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Hg(CN)2, HgBr₂ / CH₂Cl₂ / Ambient temperature

2: 74 percent / thiourea / ethanol / 6 h / Heating

With mercury(II) cyanide; thiourea; mercury dibromide; In ethanol; dichloromethane;
DOI:10.1021/jm00364a032

Reference yield:

: 80851-32-7
6-deoxy-2,3,5-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl bromide

: 86527-22-2
9-<6'-deoxy-2',3',5'-tris-O-(p-nitrobenzoyl)-α-L-talofuranosyl>-6-thiopurine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Hg(CN)2, HgBr₂ / CH₂Cl₂ / Ambient temperature

2: 74 percent / thiourea / ethanol / 6 h / Heating

With mercury(II) cyanide; thiourea; mercury dibromide; In ethanol; dichloromethane;
DOI:10.1021/jm00364a032