(2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate

Base Information

Chemical Name:(2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate
CAS No.:1300013-97-1
Molecular Formula:C₂₁H₂₃FN₂O₈
Molecular Weight:450.421
Hs Code.:

Synonyms:(2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate

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Chemical Property of (2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate

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Technology Process of (2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate

There total 2 articles about (2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 133860-74-9
ethyl 2-fluoro-3-(4'-nitrophenyl)-3-oxo-propanoate

: 479423-46-6
(1-furan-2-ylmethylidene)carbamic acid tert-butyl ester

: 1300013-97-1
(2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate

Guidance literature:: With C₃₇H₃₁F₆N₃S; In diethyl ether; at 20 ℃; for 36h; optical yield given as %de; enantioselective reaction;
DOI:10.1055/s-0030-1259319

Reference yield:

: 133860-74-9
ethyl 2-fluoro-3-(4'-nitrophenyl)-3-oxo-propanoate

: 479423-46-6
(1-furan-2-ylmethylidene)carbamic acid tert-butyl ester

: 1300013-97-1
(2S,3S)-ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate

: ethyl 2-(4-nitrobenzoyl)-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-furanyl)propanoate

Guidance literature:: With C₃₇H₃₁F₆N₃S; In diethyl ether; at 20 ℃; for 36h; optical yield given as %ee; enantioselective reaction;
DOI:10.5012/bkcs.2011.32.4.1195