1-(4-nonylphenyl)-1-chloroethene

Base Information

• Chemical Name: 1-(4-nonylphenyl)-1-chloroethene
• CAS No.: 123501-85-9
• Molecular Formula: C₁₇H₂₅Cl
• Molecular Weight: 264.838
• Mol file: 123501-85-9.mol

Synonyms:1-(4-nonylphenyl)-1-chloroethene

Chemical Property of 1-(4-nonylphenyl)-1-chloroethene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-(4-nonylphenyl)-1-chloroethene

There total 2 articles about 1-(4-nonylphenyl)-1-chloroethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

p-nonyl acetophenone (37593-05-8) → 1-(4-nonylphenyl)-1-chloroethene (123501-85-9)

Guidance literature:

With phosphorus pentachloride; at 20 ℃; for 12h;

DOI:10.1080/15421400390213311

Reference yield:

n-nonylbenzene (1081-77-2) → 1-(4-nonylphenyl)-1-chloroethene (123501-85-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 59 percent / AlCl₃ / CCl₄ / 2 h / 0 - 20 °C

2: 64 percent / PCl₅ / 12 h / 20 °C

With aluminium trichloride; phosphorus pentachloride; In tetrachloromethane;

DOI:10.1080/15421400390213311

Reference yield: 50.0%

1-(4-nonylphenyl)-1-chloroethene (123501-85-9) → 1-ethynyl-4-nonylbenzene (123501-86-0)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol; at 110 ℃; for 36h;

DOI:10.1080/15421400390213311

upstream raw materials:

p-nonyl acetophenone

n-nonylbenzene

Downstream raw materials:

1-ethynyl-4-nonylbenzene