11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine

Base Information

Chemical Name:11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine
CAS No.:863332-67-6
Molecular Formula:C₃₉H₄₆N₂OSi₂
Molecular Weight:614.978
Hs Code.:

Synonyms:11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine

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Technology Process of 11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine

There total 2 articles about 11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1025-08-7
(R)-methyl(1-naphthyl)phenylsilane

: 518028-05-2
9-O-(trimethylsilyl)cinchonidine

: 863332-67-6
11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine

Guidance literature:: chloroplatinic acid 1,1,3,3-tetramethyl-1,3-divinyldisiloxane complex; In toluene; at 80 - 90 ℃; for 4h;
DOI:10.1002/ejoc.200500161

Reference yield:

: 118-10-5,485-70-1,485-71-2,550-54-9,40134-63-2,72402-55-2,72402-56-3
cinchonidine

: 863332-67-6
11-[(R)-methyl(1-naphthyl)phenylsilyl]-9-O-(trimethylsilyl)-10,11-dihydrocinchonidine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N / tetrahydrofuran

2: 38 percent / Karstedt's catalyst / toluene / 4 h / 80 - 90 °C

With triethylamine; chloroplatinic acid 1,1,3,3-tetramethyl-1,3-divinyldisiloxane complex; In tetrahydrofuran; toluene;
DOI:10.1002/ejoc.200500161