N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester

Base Information

• Chemical Name: N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester
• CAS No.: 109978-00-9
• Molecular Formula: C₃₇H₃₈INO₁₂
• Molecular Weight: 815.613

Synonyms:N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester

Chemical Property of N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester

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Technology Process of N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester

There total 3 articles about N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-(9-fluorenylmethyloxycarbonyl)-L-serine benzyl ester (118358-66-0,73724-46-6) + triacetyl-D-galactal (4098-06-0) → Fmoc-Ser(3,4,6-Tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-OBzl (109978-00-9)

Guidance literature:

With N-iodo-succinimide; In dichloromethane; acetonitrile; Ambient temperature;

Reference yield: 70.0%

Fmoc-Ser-OBzl (73724-46-6) + triacetyl-D-galactal (4098-06-0) → 3-((2S,3R,4S,5S,6R)-4,5-Diacetoxy-6-acetoxymethyl-3-iodo-tetrahydro-pyran-2-yloxy)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzyl ester (109977-95-9,109978-00-9) + N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester (109978-00-9)

Guidance literature:

With N-iodo-succinimide; In acetonitrile; Ambient temperature;

Reference yield: 70.0%

Fmoc-Ser-OBzl (73724-46-6) + triacetyl-D-galactal (4098-06-0) → 3-((2S,3R,4S,5S,6R)-4,5-Diacetoxy-6-acetoxymethyl-3-iodo-tetrahydro-pyran-2-yloxy)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzyl ester (109977-95-9,109978-00-9) + N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-2-iod-α-D-talopyranosyl)-L-serin-benzylester (109978-00-9)

Guidance literature:

With N-iodo-succinimide; In acetonitrile; Ambient temperature;

upstream raw materials:

Fmoc-Ser-OBzl

triacetyl-D-galactal

N-(9-fluorenylmethyloxycarbonyl)-L-serine benzyl ester

Downstream raw materials:

N-(9-Fluorenylmethoxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-desoxy-α-D-lyxo-hexopyranosyl)-L-serin-benzylester

Fmoc-Ser-(3,4,6-Tri-O-acetyl-2-desoxy-α-D-galactosyl)-OBzl

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