C₃₆H₅₄FN₃O₉SSi

Base Information

Chemical Name:C₃₆H₅₄FN₃O₉SSi
CAS No.:1402742-42-0
Molecular Formula:C₃₆H₅₄FN₃O₉SSi
Molecular Weight:751.989
Hs Code.:

C<sub>36</sub>H<sub>54</sub>FN<sub>3</sub>O<sub>9</sub>SSi

Synonyms:C₃₆H₅₄FN₃O₉SSi

Suppliers and Price of C₃₆H₅₄FN₃O₉SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₆H₅₄FN₃O₉SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₆H₅₄FN₃O₉SSi

There total 6 articles about C₃₆H₅₄FN₃O₉SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402742-17-9
C₂₈H₃₆FN₃O₇S

: 102191-92-4
tert-butyldimethylsiloxyacetaldehyde

: 1402742-42-0
C₃₆H₅₄FN₃O₉SSi

Guidance literature:: C₂₈H₃₆FN₃O₇S; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

tert-butyldimethylsiloxyacetaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 3h;

Reference yield:

: 1402742-11-3
C₁₅H₁₃FO₂

: 1402742-42-0
C₃₆H₅₄FN₃O₉SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

2.2: 3 h / -78 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 - 25 °C

4.1: mercaptoacetic acid; trifluoroacetic acid / 16 h / 0 - 25 °C

4.2: pH 8

5.1: acetonitrile / 16 h / 60 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 30 °C

7.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C

7.2: 3 h / -78 °C

With hydrogenchloride; dmap; titanium(IV) tetraethanolate; n-butyllithium; mercaptoacetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; acetonitrile;

Reference yield:

: 1402742-12-4
C₁₉H₂₂FNO₂S

: 1402742-42-0
C₃₆H₅₄FN₃O₉SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 3 h / -78 °C

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 - 25 °C

3.1: mercaptoacetic acid; trifluoroacetic acid / 16 h / 0 - 25 °C

3.2: pH 8

4.1: acetonitrile / 16 h / 60 °C

5.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 30 °C

6.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C

6.2: 3 h / -78 °C

With hydrogenchloride; dmap; n-butyllithium; mercaptoacetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; acetonitrile;