3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

Base Information

Chemical Name:3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one
CAS No.:213014-33-6
Molecular Formula:C₂₃H₂₇NO₃
Molecular Weight:365.472
Hs Code.:

Synonyms:3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

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Technology Process of 3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

There total 6 articles about 3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Hydroxy-3-(3-nitro-benzyl)-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

: 213014-33-6
3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 2h;
DOI:10.1021/jm9802158

Reference yield:

: 29898-25-7
1-phenylhexan-3-one

: 213014-33-6
3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH, 2.) n-BuLi, 3.) 6 N HCl

2: aq. NaOH / methanol

3: AlCl₃ / tetrahydrofuran / 2 h / Ambient temperature

4: sodium cyanoborohydride / methanol / 1 h / 0 °C

5: ammonium formate / 10percent Pd/C / methanol / 2 h

With hydrogenchloride; sodium hydroxide; n-butyllithium; aluminium trichloride; ammonium formate; sodium hydride; sodium cyanoborohydride; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm9802158

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 213014-33-6
3-(3-Amino-benzyl)-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / tetrahydrofuran / 2 h / Ambient temperature

2: sodium cyanoborohydride / methanol / 1 h / 0 °C

3: ammonium formate / 10percent Pd/C / methanol / 2 h

With aluminium trichloride; ammonium formate; sodium cyanoborohydride; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm9802158