ptelatoside-A hexaacetate

Base Information

Chemical Name:ptelatoside-A hexaacetate
CAS No.:91067-43-5
Molecular Formula:C₃₁H₃₈O₁₆
Molecular Weight:666.633
Hs Code.:

Synonyms:ptelatoside-A hexaacetate

Suppliers and Price of ptelatoside-A hexaacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ptelatoside-A hexaacetate

Chemical Property:

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Technology Process of ptelatoside-A hexaacetate

There total 6 articles about ptelatoside-A hexaacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91067-45-7
p-ethylphenyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside

: 91067-43-5
ptelatoside-A hexaacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Hg(CN)2-HgBr₂ / acetonitrile / 1 h / Ambient temperature

2: 1.) Br₂, NaHCO₃, 2.) AcONa / 1.) CHCl₃, irradiation, r.t., 30 min, 2.) AcOH, reflux, 40 h

With bromine; sodium acetate; mercury(II) cyanide; sodium hydrogencarbonate; mercury dibromide; In acetonitrile;
DOI:10.1246/cl.1984.397

Reference yield:

: 3068-31-3
1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose

: 91067-43-5
ptelatoside-A hexaacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Hg(CN)2, HgBr₂ / acetonitrile / 1 h / Ambient temperature

2: 1.) NaHCO₃, Br₂; 2.) NaOAc / 1.) CHCl₃,20 deg C, 55 min; 2.) AcOH, reflux, 40h

With bromine; sodium acetate; mercury(II) cyanide; sodium hydrogencarbonate; mercury dibromide; In acetonitrile;
DOI:10.1016/S0040-4020(01)87703-6

Reference yield:

: (2S,3R,4S,5S,6R)-2-(4-Ethyl-phenoxy)-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

: 91067-43-5
ptelatoside-A hexaacetate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 3 h / Ambient temperature

2: acetic acid; H₂O / 0.83 h / 100 °C

3: 86 percent / Hg(CN)2-HgBr₂ / acetonitrile / 1 h / Ambient temperature

4: 1.) Br₂, NaHCO₃, 2.) AcONa / 1.) CHCl₃, irradiation, r.t., 30 min, 2.) AcOH, reflux, 40 h

With pyridine; bromine; sodium acetate; mercury(II) cyanide; sodium hydrogencarbonate; mercury dibromide; In water; acetic acid; acetonitrile;
DOI:10.1246/cl.1984.397