[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]⁽¹⁺⁾*Cl^(1-)=[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]Cl

Base Information

• Chemical Name: [(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]⁽¹⁺⁾*Cl^(1-)=[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]Cl
• CAS No.: 96213-76-2
• Molecular Formula: CH₂Cl₂*C₃₆H₃₂ClNOP₂Re*Cl
• Molecular Weight: 898.65

Synonyms:[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]⁽¹⁺⁾*Cl^(1-)=[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]Cl

Chemical Property of [(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]⁽¹⁺⁾*Cl^(1-)=[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]Cl

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Technology Process of [(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]⁽¹⁺⁾*Cl^(1-)=[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]Cl

There total 2 articles about [(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]⁽¹⁺⁾*Cl^(1-)=[(C₅H₅)Re(P(C₆H₅)3)(P(CH₂Cl)(C₆H₅)2)(NO)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

(η5-C5H5)Re(NO)(P(C6H5)3)P(C6H5)2 (96213-75-1) → (C5H5)Re(NO)(P(C6H5)3)P(C6H5)2CH2Cl(1+)*Cl(1-)*CH2Cl2={(C5H5)Re(NO)(P(C6H5)3)P(C6H5)2CH2Cl}Cl*CH2Cl2 (96213-76-2)

Guidance literature:

With CH₂Cl₂; In dichloromethane; (C5H5)Re(NO)PpPPh2 stirred in CH2Cl2 for 3 h; after addn. of ether formed ppt. filtered, washed with ether and dried in vacuo at 56 ° C; elem. anal.;

DOI:10.1021/ja00216a015

Reference yield: 79.0%

(η5-C5H5)Re(NO)(P(C6H5)3)P(C6H5)2 (96213-75-1) → [(C5H5)Re(P(C6H5)3)(P(CH2Cl)(C6H5)2)(NO)](1+)*Cl(1-)=[(C5H5)Re(P(C6H5)3)(P(CH2Cl)(C6H5)2)(NO)]Cl (96213-76-2)

Guidance literature:

With CH₂Cl₂; at 25 °C, 2 h; elem. anal.;

DOI:10.1021/ja00297a050

upstream raw materials:

(η5-C5H5)Re(NO)(P(C6H5)3)P(C6H5)2

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