(1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol

Base Information

• Chemical Name: (1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol
• CAS No.: 163114-94-1
• Molecular Formula: C₁₆H₁₃N₅O₂
• Molecular Weight: 307.312
• Mol file: 163114-94-1.mol

Synonyms:(1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol

Chemical Property of (1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol

There total 2 articles about (1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

guanazole (1455-77-2) + salicylaldehyde (90-02-8) → (1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol (163114-94-1)

Guidance literature:

In neat (no solvent); at 30 ℃; for 0.5h;

DOI:10.1016/j.molstruc.2020.129444

Reference yield:

salicylaldehyde (90-02-8) → (1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol (163114-94-1)

Guidance literature:

Reference yield: 79.0%

(1H-1,2,4-triazole-3,5-diyl)bis(azanylylidene)bis(methanylylidene)diphenol (163114-94-1) + silver nitrate → Ag(1+)*N3C2(NCHC6H4OH)2(1-)=Ag(N3C2(NCHC6H4OH)2)

Guidance literature:

With Et₃N; In acetonitrile; under N2; ligand and Et3N added to soln. of AgNO3 in MeCN; stirred at room temp. for 2 h; filtered; ppt. washed with MeCN; elem. anal.;

DOI:10.1016/j.jorganchem.2008.02.014

upstream raw materials:

guanazole

salicylaldehyde

Downstream raw materials:

(Cu(N₃C₂(NCHC₆H₄OH)2)(CH₃CN))2

(Cu(N₃C₂(NCHC₆H₄OH)2)(CO))2