4-Isoxazolecarboxylicacid,3-methyl-5-(o-nitrophenyl)-,methylester(8CI)

Base Information

• Chemical Name: 4-Isoxazolecarboxylicacid,3-methyl-5-(o-nitrophenyl)-,methylester(8CI)
• CAS No.: 24290-22-0
• Molecular Formula: C₁₂H₁₀N₂O₅
• Molecular Weight: 262.222
• Mol file: 24290-22-0.mol

Synonyms:4-Isoxazolecarboxylicacid, 3-methyl-5-(o-nitrophenyl)-, methyl ester (8CI)

Chemical Property of 4-Isoxazolecarboxylicacid,3-methyl-5-(o-nitrophenyl)-,methylester(8CI)

Chemical Property:

• PSA: 98.15000
• LogP: 2.86800

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Isoxazolecarboxylicacid,3-methyl-5-(o-nitrophenyl)-,methylester(8CI)

There total 1 articles about 4-Isoxazolecarboxylicacid,3-methyl-5-(o-nitrophenyl)-,methylester(8CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-nitro-benzoyl)-3-oxo-butyric acid methyl ester (91396-68-8) → 3-methyl-5-(2-nitro-phenyl)-isoxazole-4-carboxylic acid methyl ester (24290-22-0)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; In ethanol; for 2h; Heating;

DOI:10.1039/j39690002207

Reference yield:

3-methyl-5-(2-nitro-phenyl)-isoxazole-4-carboxylic acid methyl ester (24290-22-0) → 5-Hydroxy-3-methyl-5H-isoxazolo<4,5-c>chinolin-4-on (21201-45-6)

Guidance literature:

With sodium tetrahydroborate; palladium on activated charcoal; In 1,4-dioxane; water;

DOI:10.1039/j39690002207

upstream raw materials:

2-(2-nitro-benzoyl)-3-oxo-butyric acid methyl ester

Downstream raw materials:

5-Hydroxy-3-methyl-5H-isoxazolo<4,5-c>chinolin-4-on

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