(2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal

Base Information

Chemical Name:(2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal
CAS No.:104976-70-7
Molecular Formula:C₃₀H₃₄O₆
Molecular Weight:490.596
Hs Code.:

Synonyms:(2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal

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Chemical Property of (2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal

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Technology Process of (2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal

There total 7 articles about (2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 908836-17-9
(2S,3R,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butan-1-ol

: 104976-70-7
(2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal

Guidance literature:: (2S,3R,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butan-1-ol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 - -65 ℃; for 1h;

With triethylamine; In dichloromethane; at -65 - 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2016.03.064

Reference yield: 71.0%

: 104976-69-4
2,3,4-Tri-O-benzyl-5,6-O-isopropyliden-D-glucose-diethyldithioacetal

: 104976-70-7
(2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal

Guidance literature:: With mercury dichloride; mercury(II) oxide; In water; acetonitrile;

Reference yield: 61.0%

: 1049006-94-1
C₅₉H₆₆O₁₁

: 104976-70-7
(2R,3S,4R)-2,3,4-tris(benzyloxy)-4-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)butanal

: 103597-24-6
methyl 2,3,4-tri-O-benzyl-L-glycero-α-D-gluco-heptopyranoside

Guidance literature:: C₅₉H₆₆O₁₁; With ozone; In methanol; dichloromethane; at -78 ℃;

With dimethylsulfide; In methanol; dichloromethane; at 20 ℃; for 0.25h;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.tetasy.2008.05.010