{[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane

Base Information

Chemical Name:{[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane
CAS No.:947770-26-5
Molecular Formula:C₂₆H₄₅NSi₃
Molecular Weight:455.907
Hs Code.:

Synonyms:{[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane

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Chemical Property of {[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane

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Technology Process of {[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane

There total 1 articles about {[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 2-(2,6-diisopropylphenyl)pyridine

: 86932-21-0
bromodimethylsilylbis(trimethylsilyl)methane

: 947770-26-5
{[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane

Guidance literature:: 2-(2,6-diisopropylphenyl)pyridine; With n-butyllithium; 2-(N,N-dimethylamino)ethanol; In hexane; at 0 ℃; for 1h;

bromodimethylsilylbis(trimethylsilyl)methane; In hexane; at -78 - 20 ℃; for 17h; Further stages.;
DOI:10.1139/V07-063

Reference yield: 86.0%

: 947770-26-5
{[6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl}bis(trimethylsilyl)methane

: 917-54-4
methyllithium

: 1184-58-3
dimethylaluminum chloride

: 947770-22-1
(([6-(2,6-diisopropylphenyl)pyrid-2-yl]dimethylsilyl)bis(trimethylsilyl)methyl)dimethylaluminum

Guidance literature:: In tetrahydrofuran; hexane; byproducts: CH4, LiCl; Schlenk technique; LiCH3 in THF/cumene added dropwise to pyridyl-compd. in THF at room temp., stirred for 4 h, Me2AlCl in hexane slowly added at-78°C, stirred at room temp. overnight; evapn. under vac., solid extd. with ether, extract filtered, filtrate evapd. under vac., residue dissolved in warm hexane, crystn. at -30°C; elem. anal.;
DOI:10.1139/V07-063