1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine

Base Information

Chemical Name:1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine
CAS No.:182060-48-6
Molecular Formula:C₂₁H₄₂NPSi
Molecular Weight:367.63
Hs Code.:

1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ<sup>5</sup>-phosphanimine

Synonyms:1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine

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Chemical Property of 1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine

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Technology Process of 1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine

There total 1 articles about 1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 4648-54-8
trimethylsilylazide

: 2622-14-2
tricyclohexylphosphine

: 182060-48-6
1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine

Guidance literature:: for 10h; Reflux;

Reference yield: 94.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 182060-48-6
1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine

: 222054-54-8
[CpTiCl₂(NPCy₃)]

Guidance literature:: In benzene; (N2); using Schlenk techniques; addn. of benzene to Cy3PNSiMe3 (1 equiv.) and CpTiCl3 (1 equiv.); heating at 80°C for 4 h; cooling, removal of volatiles, elem. anal.;
DOI:10.1021/om020954t

Reference yield: 93.0%

: (tert-butylcyclopentadienyl)titanium(IV) trichloride

: 182060-48-6
1,1,1-tricyclohexyl-N-(trimethylsilyl)-λ⁵-phosphanimine

: 222054-56-0
[(η5-C5H4C(CH3)3)TiCl2(NPCy3)]

Guidance literature:: In benzene; (N2); using Schlenk techniques; addn. of benzene to Cy3PNSiMe3 (1 equiv.) and ((t-Bu)C5H4)TiCl3 (1 equiv.); heating at 80°C for 4 h; cooling, removal of volatiles, elem. anal.;
DOI:10.1021/om020954t