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C30H44O6Si

Base Information
  • Chemical Name:C30H44O6Si
  • CAS No.:1373634-24-2
  • Molecular Formula:C30H44O6Si
  • Molecular Weight:528.761
  • Hs Code.:
C<sub>30</sub>H<sub>44</sub>O<sub>6</sub>Si

Synonyms:C30H44O6Si

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Chemical Property of C30H44O6Si
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Technology Process of C30H44O6Si

There total 11 articles about C30H44O6Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; hexane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol300672q
Guidance literature:
Multi-step reaction with 10 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.17 h / 0 - 20 °C / Inert atmosphere
1.2: 0.67 h / 20 °C / Inert atmosphere
2.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
3.1: sodium periodate; sodium hydrogencarbonate / dichloromethane; water / 20 °C / Inert atmosphere
4.1: sodium tetrahydroborate / methanol / 0.17 h / 0 °C / Inert atmosphere
5.1: Crabtree's catalyst; hydrogen / dichloromethane / 0 °C / Inert atmosphere
6.1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
7.1: methanol; potassium carbonate / 2 h / 20 °C / Inert atmosphere
8.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C / Inert atmosphere
9.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere
9.2: 0 - 20 °C / Inert atmosphere
10.1: water; dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; hexane / 0.5 h / 20 °C / Inert atmosphere
With 1H-imidazole; methanol; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; Crabtree's catalyst; water; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; 4-methylmorpholine N-oxide; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol300672q
Guidance literature:
Multi-step reaction with 9 steps
1.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
2.1: sodium periodate; sodium hydrogencarbonate / dichloromethane; water / 20 °C / Inert atmosphere
3.1: sodium tetrahydroborate / methanol / 0.17 h / 0 °C / Inert atmosphere
4.1: Crabtree's catalyst; hydrogen / dichloromethane / 0 °C / Inert atmosphere
5.1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
6.1: methanol; potassium carbonate / 2 h / 20 °C / Inert atmosphere
7.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C / Inert atmosphere
8.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere
8.2: 0 - 20 °C / Inert atmosphere
9.1: water; dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; hexane / 0.5 h / 20 °C / Inert atmosphere
With 1H-imidazole; methanol; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; Crabtree's catalyst; water; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; 4-methylmorpholine N-oxide; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol300672q
upstream raw materials:

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