9-phenylsulfonyl nerolidol

Base Information

Chemical Name:9-phenylsulfonyl nerolidol
CAS No.:132407-54-6
Molecular Formula:C₂₁H₃₀O₃S
Molecular Weight:362.533
Hs Code.:

Synonyms:9-phenylsulfonyl nerolidol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-phenylsulfonyl nerolidol

Chemical Property:

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Technology Process of 9-phenylsulfonyl nerolidol

There total 5 articles about 9-phenylsulfonyl nerolidol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 132407-53-5
(3R)-9-phenylsulfonyl nerolidol TBDMS ether

: 132407-54-6
9-phenylsulfonyl nerolidol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 18h; Heating;
DOI:10.1016/S0040-4039(00)97296-4

Reference yield:

: 126-91-0
linalool

: 132407-54-6
9-phenylsulfonyl nerolidol

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 1.) SeO₂, 2.) NaBH₄ / 1.) EtOH, reflux, 4 h

3: 48 percent / triphenylphosphine, CCl₄ / 4 h / Heating

4: 1.) n-butyl lithium / 1.) a) -78 deg C, 0.5 h, b) 0.5 h, r.t. 2.) THF, -78 deg C, 0.5 h

5: 82 percent / (n-Bu)4NF / tetrahydrofuran / 18 h / Heating

With 2,6-dimethylpyridine; tetrachloromethane; sodium tetrahydroborate; n-butyllithium; selenium(IV) oxide; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)97296-4

Reference yield:

: 132407-50-2
(R)-tert-butyl((3,7-dimethylocta-1,6-dien-3-yl)oxy)dimethylsilane

: 132407-54-6
9-phenylsulfonyl nerolidol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) SeO₂, 2.) NaBH₄ / 1.) EtOH, reflux, 4 h

2: 48 percent / triphenylphosphine, CCl₄ / 4 h / Heating

3: 1.) n-butyl lithium / 1.) a) -78 deg C, 0.5 h, b) 0.5 h, r.t. 2.) THF, -78 deg C, 0.5 h

4: 82 percent / (n-Bu)4NF / tetrahydrofuran / 18 h / Heating

With tetrachloromethane; sodium tetrahydroborate; n-butyllithium; selenium(IV) oxide; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)97296-4