2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline

Base Information

• Chemical Name: 2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline
• CAS No.: 305344-42-7
• Molecular Formula: C₃₈H₄₀N₂O₄
• Molecular Weight: 588.747

Synonyms:2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline

Chemical Property of 2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline

Chemical Property:

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Technology Process of 2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline

There total 1 articles about 2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

methyllithium (917-54-4) + 2-methyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline → 2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline (305344-42-7)

Guidance literature:

methyllithium; 2-methyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline; In toluene; at 2 - 5 ℃; for 3h;

With water;

With manganese(IV) oxide; In dichloromethane; Further stages.;

DOI:10.1021/ol006137b

Reference yield: 89.0%

2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline (305344-42-7) → 2,9-dimethyl-3,8-di(p-formylphenyl)-1,10-phenanthroline

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 50 ℃; for 24h;

DOI:10.1021/ol006137b

Reference yield:

2,9-dimethyl-3,8-di[p-(5,5-dimethyl-1,3-dioxan-2-yl)]phenyl-1,10-phenanthroline (305344-42-7) → 2,9-dimethyl-3,8-di(p-carboxyphenyl)-1,10-phenanthroline hydrochloride

Guidance literature:

Multi-step reaction with 2 steps

1.1: 89 percent / HCl / H₂O; tetrahydrofuran / 24 h / 50 °C

2.1: KMnO₄ / acetone; H₂O / 2 h / 40 °C

2.2: 89 percent / HCl / H₂O / cooling

With hydrogenchloride; potassium permanganate; In tetrahydrofuran; water; acetone; 1.1: Hydrolysis / 2.1: Oxidation / 2.2: salt formation;

DOI:10.1021/ol006137b

upstream raw materials:

methyllithium

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