(2R,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine

Base Information

Chemical Name:(2R,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine
CAS No.:1258505-42-8
Molecular Formula:C₂₄H₃₁NO₉S
Molecular Weight:509.577
Hs Code.:

Synonyms:(2R,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine

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Technology Process of (2R,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine

There total 1 articles about (2R,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1258505-13-3
3,4-di-O-acetyl-1,4-anhydro-N-(2,2-diethoxycarbonylvinyl)-α-L-arabinopyranosylamine

: 106-45-6
para-thiocresol

: 1258505-42-8
(2R,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine

: 1258505-37-1
(2S,3R,4S,5S)-3,4-di-acetoxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethyl-2-p-tolylthiopyrrolidine

Guidance literature:: 3,4-di-O-acetyl-1,4-anhydro-N-(2,2-diethoxycarbonylvinyl)-α-L-arabinopyranosylamine; With boron trifluoride diethyl etherate; In diethyl ether; at 20 ℃; Molecular sieve; Inert atmosphere;

para-thiocresol; In diethyl ether; at 20 ℃; for 1h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.09.065